Technology Process of C20H16Cl2N2
There total 4 articles about C20H16Cl2N2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dimethylaluminum chloride;
In
hexane; toluene;
at 20 - 150 ℃;
for 0.5h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 0.5 h / 160 °C / Microwave irradiation
2: tert.-butylnitrite / dimethyl sulfoxide / 1.5 h / 50 °C
3: dimethylaluminum chloride / hexane; toluene / 0.5 h / 20 - 150 °C / Microwave irradiation
With
tert.-butylnitrite; dimethylaluminum chloride; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; hexane; water; dimethyl sulfoxide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 0.5 h / 160 °C / Microwave irradiation
2: tert.-butylnitrite / dimethyl sulfoxide / 1.5 h / 50 °C
3: dimethylaluminum chloride / hexane; toluene / 0.5 h / 20 - 150 °C / Microwave irradiation
With
tert.-butylnitrite; dimethylaluminum chloride; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; hexane; water; dimethyl sulfoxide; toluene;