2-(2,4-dimethylphenyl)-1,3-benzothiazole

Base Information

• Chemical Name: 2-(2,4-dimethylphenyl)-1,3-benzothiazole
• CAS No.: 902086-26-4
• Molecular Formula: C₁₅H₁₃NS
• Molecular Weight: 239.341
• Mol file: 902086-26-4.mol

Synonyms:2-(2,4-dimethylphenyl)-1,3-benzothiazole

Chemical Property of 2-(2,4-dimethylphenyl)-1,3-benzothiazole

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-(2,4-dimethylphenyl)-1,3-benzothiazole

There total 7 articles about 2-(2,4-dimethylphenyl)-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C15H16IN (1038731-86-0) → 2-(2,4-dimethylphenyl)-1,3-benzothiazole (902086-26-4)

Guidance literature:

With potassium sulfide; N,N,N,N,-tetramethylethylenediamine; copper(I) bromide; In 1-methyl-pyrrolidin-2-one; for 24h; Sealed tube; Heating;

DOI:10.1021/ol403638d

Reference yield: 83.0%

o-nitroiodobenzene (609-73-4) + 2,4-dimethylbenzaldehyde (15764-16-6) → 2-(2,4-dimethylphenyl)-1,3-benzothiazole (902086-26-4)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; sodiumsulfide nonahydrate; In acetic acid; at 100 ℃; for 12h; Sealed tube;

DOI:10.1055/s-0032-1318304

Reference yield: 81.0%

2,4-dimethylbenzaldehyde (15764-16-6) + 2-amino-benzenethiol (137-07-5) → 2-(2,4-dimethylphenyl)-1,3-benzothiazole (902086-26-4)

Guidance literature:

With air; In dimethyl sulfoxide; at 60 ℃; for 6h;

DOI:10.1055/s-0035-1561575

upstream raw materials:

1,3-Benzothiazole

2,4-dimethylbenzaldehyde

o-nitroiodobenzene

C₁₅H₁₆IN