1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione

Base Information

• Chemical Name: 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione
• CAS No.: 123100-06-1
• Molecular Formula: C₁₅H₁₂ClN₅S
• Molecular Weight: 329.813
• Mol file: 123100-06-1.mol

Synonyms:1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione

Chemical Property of 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione

There total 3 articles about 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.7%

2-(Benzylthio)-1-(2-chlorophenyl)-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione (123100-05-0) → 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione (123100-06-1)

Guidance literature:

With hydrazine hydrate; In benzene; for 8h;

DOI:10.1021/je00059a026

Reference yield:

S-Benzyl-N-(2-chlorophenyl)isothiourea (89070-01-9) → 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione (123100-06-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 56.3 percent / acetone

2: 63.7 percent / hydrazine hydrate / benzene / 8 h

With hydrazine hydrate; In acetone; benzene;

DOI:10.1021/je00059a026

Reference yield:

Benzoyl isothiocyanate (532-55-8) → 1-(2-Chlorophenyl)-2-hydrazino-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione (123100-06-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 56.3 percent / acetone

2: 63.7 percent / hydrazine hydrate / benzene / 8 h

With hydrazine hydrate; In acetone; benzene;

DOI:10.1021/je00059a026

upstream raw materials:

2-(Benzylthio)-1-(2-chlorophenyl)-4-phenyl-1,6-dihydro-1,3,5-triazine-6-thione

S-Benzyl-N-(2-chlorophenyl)isothiourea

Benzoyl isothiocyanate

Downstream raw materials:

C₁₆H₁₃ClN₆S₂

C₂₂H₁₆Cl₂N₆S₂

C₂₃H₁₉ClN₆S₂

C₂₂H₁₆Cl₂N₆S₂