1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

Base Information

Chemical Name:1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite
CAS No.:122901-30-8
Molecular Formula:C₄₅H₄₅Cl₃N₄O₇
Molecular Weight:860.234
Hs Code.:

Synonyms:1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

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Chemical Property of 1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

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Technology Process of 1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

There total 5 articles about 1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 122901-28-4
1L-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-2,3-didesoxy-2,3-<(2,2,2-trichloroethoxy)carbonyl>epimino-epi-inosite

: 122901-30-8
1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

Guidance literature:: With sodium azide; ammonium chloride; In 2-methoxy-ethanol; water; at 110 ℃; for 20h;

Reference yield:

: 106989-01-9
1L-2-azido-1,4,5,6-tetra-O-benzyl-2-desoxy-4-C-(benzyloxymethyl)-muco-inosit

: 122901-30-8
1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / NaBH₄ / 4 percent NiCl₂ / ethanol

2: 95 percent / K₂CO₃ / dioxane; H₂O / 0.33 h

3: 97 percent / pyridine / CH₂Cl₂ / 1.5 h / -40 °C

4: 73 percent / NaN₃ / dimethylformamide / 4 h / Ambient temperature

5: 55 percent / NaN₃, NH₄Cl, / H₂O; 2-methoxy-ethanol / 20 h / 110 °C

With pyridine; sodium tetrahydroborate; sodium azide; potassium carbonate; ammonium chloride; nickel dichloride; In 1,4-dioxane; ethanol; dichloromethane; 2-methoxy-ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 122901-18-2
1L-2-amino-1,4,5,6-tetra-O-benzyl-4-C-bezyloxymethyl-2-desoxy-muco-inosite

: 122901-30-8
1L-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-1,6-didesoxy-1-<(2,2,2-trichloroethoxy)carbonylamino>-myo-inosite

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / K₂CO₃ / dioxane; H₂O / 0.33 h

2: 97 percent / pyridine / CH₂Cl₂ / 1.5 h / -40 °C

3: 73 percent / NaN₃ / dimethylformamide / 4 h / Ambient temperature

4: 55 percent / NaN₃, NH₄Cl, / H₂O; 2-methoxy-ethanol / 20 h / 110 °C

With pyridine; sodium azide; potassium carbonate; ammonium chloride; In 1,4-dioxane; dichloromethane; 2-methoxy-ethanol; water; N,N-dimethyl-formamide;