2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

Base Information

Chemical Name:2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine
CAS No.:1286775-78-7
Molecular Formula:C₃₈H₃₂ClN₂P₃
Molecular Weight:645.06
Hs Code.:

Synonyms:2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

Chemical Property:

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Technology Process of 2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

There total 3 articles about 2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 158363-40-7
N¹,N²-bis(2-(diphenylphosphanyl)phenyl)ethane-1,2-diamine

: 1286775-78-7
2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

Guidance literature:: With triethylamine; phosphorus trichloride; In tetrahydrofuran;
DOI:10.1039/c0cc05739h

Reference yield:

: 1286775-76-5
N,N-bis(2-fluorophenyl)ethane-1,2-diamine

: 1286775-78-7
2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-dioxane / 48 h / Reflux; Inert atmosphere

2: triethylamine; phosphorus trichloride / tetrahydrofuran

With triethylamine; phosphorus trichloride; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/c0cc05739h

Reference yield:

: 348-54-9
2-Fluoroaniline

: 1286775-78-7
2-chloro-1,3-bis(2-(diphenylphosphino)phenyl)-1,3,2-diazaphospholidine

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / 4 h / 130 °C

2: 1,4-dioxane / 48 h / Reflux; Inert atmosphere

3: triethylamine; phosphorus trichloride / tetrahydrofuran

With triethylamine; N-ethyl-N,N-diisopropylamine; phosphorus trichloride; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/c0cc05739h