diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

Base Information

Chemical Name:diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate
CAS No.:1121858-36-3
Molecular Formula:C₂₆H₃₀N₃O₈P
Molecular Weight:543.513
Hs Code.:

Synonyms:diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

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Chemical Property of diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

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Technology Process of diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

There total 1 articles about diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1121858-32-9
diethyl 3-(4-oxopiperidin-1-yl)propylphosphonate

: 555-16-8
4-nitrobenzaldehdye

: 1121858-36-3
diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

Guidance literature:: diethyl 3-(4-oxopiperidin-1-yl)propylphosphonate; 4-nitrobenzaldehdye; With hydrogenchloride; acetic acid;

With water; potassium carbonate; In dichloromethane; for 0.166667h; pH=8 - 9;
DOI:10.1016/j.ejmech.2008.10.019

Reference yield: 81.0%

: 1121858-36-3
diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

: 3-[(3E,5E)-3,5-bis(4-nitrobenzylidene)-4-oxo-1-piperidinyl]propylphosphonic acid hydrobromide

Guidance literature:: diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate; With trimethylsilyl bromide; In chloroform; at 20 ℃; for 24h;

With water; In methanol;
DOI:10.1016/j.ejmech.2008.10.019

Reference yield:

: 1121858-36-3
diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate

: disodium 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]propylphosphonate

Guidance literature:: diethyl 3-[3,5-bis(4-nitrobenzylidene)-4-oxopiperidin-1-yl]-propylphosphonate; With trimethylsilyl bromide; In chloroform; at 20 ℃; for 24h;

With sodium hydroxide; In ethanol; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2008.10.019