methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

Base Information

Chemical Name:methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate
CAS No.:1282534-48-8
Molecular Formula:C₂₁H₁₈N₂O₄
Molecular Weight:362.385
Hs Code.:

Synonyms:methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

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Chemical Property of methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

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Technology Process of methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

There total 1 articles about methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 13669-42-6
3-quinolylcarboxaldehyde

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 1282534-48-8
methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

Guidance literature:: N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

3-quinolylcarboxaldehyde; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/cbic.201000597

Reference yield: 99.0%

: 1282534-48-8
methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

: 1282534-50-2
methyl (2S)-2-benzyloxycarbonylamino-3-(3-quinolyl)propanoate

Guidance literature:: With (+)-1,2-bis-[(2S,5S)-2,5-diethylphospholano]benzene (1,5-cycloctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen; In methanol; at 25 ℃; for 24h; under 3750.38 Torr; enantioselective reaction; Inert atmosphere;
DOI:10.1002/cbic.201000597

Reference yield:

: 1282534-48-8
methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(quinolin-3-yl)prop-2-enoate

: methyl N-[(benzyloxy)carbonyl]-3-quinolin-3-yl-D-alaninate

Guidance literature:: With hydrogen; [((R)-tert-butylmethylphosphino)(di-tert-butylphosphino)amine](1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In methanol; at 18 - 25 ℃; for 40h;