C₃₇H₅₁N₇O₃

Base Information

Chemical Name:C₃₇H₅₁N₇O₃
CAS No.:1220900-18-4
Molecular Formula:C₃₇H₅₁N₇O₃
Molecular Weight:641.857
Hs Code.:

C<sub>37</sub>H<sub>51</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:C₃₇H₅₁N₇O₃

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Chemical Property of C₃₇H₅₁N₇O₃

Chemical Property:

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Technology Process of C₃₇H₅₁N₇O₃

There total 13 articles about C₃₇H₅₁N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33841-56-4
(1H-tetrazol-5-ylmethyl)amine hydrobromide

: 1220904-31-3
C₃₅H₄₈N₂O₄

: 1220900-18-4
C₃₇H₅₁N₇O₃

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1220900-18-4
C₃₇H₅₁N₇O₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: potassium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 64 h / 70 °C

2.1: caesium carbonate / dichloromethane / 30 h / 42 °C

3.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

3.2: 2 h / -78 - 20 °C

3.3: 0 °C

4.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16.25 h / 0 - 20 °C

6.1: trifluoroacetic acid / dichloromethane / 4 h

7.1: triethylamine / isopropyl alcohol / 24 h / Reflux; Molecular sieve; Inert atmosphere

8.1: tert-butylhypochlorite / dichloromethane / 0.75 h

8.2: 0.75 h

9.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -10 °C

11.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 0.75 h / 100 °C / Microwave irradiation

12.1: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

13.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 3 h / 20 °C

With hydrogenchloride; methanol; tert-butylhypochlorite; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; iodine; sodium carbonate; potassium carbonate; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 70240-29-8
4-(isopropyloxycarbonyl)benzaldehyde

: 1220900-18-4
C₃₇H₅₁N₇O₃

Guidance literature:: Multi-step reaction with 12 steps

1.1: caesium carbonate / dichloromethane / 30 h / 42 °C

2.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

2.2: 2 h / -78 - 20 °C

2.3: 0 °C

3.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16.25 h / 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 4 h

6.1: triethylamine / isopropyl alcohol / 24 h / Reflux; Molecular sieve; Inert atmosphere

7.1: tert-butylhypochlorite / dichloromethane / 0.75 h

7.2: 0.75 h

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -10 °C

10.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 0.75 h / 100 °C / Microwave irradiation

11.1: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C

12.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 3 h / 20 °C

With hydrogenchloride; methanol; tert-butylhypochlorite; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; iodine; sodium carbonate; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;