5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

Base Information

Chemical Name:5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol
CAS No.:879015-67-5
Molecular Formula:C₁₇H₂₇BrO₇
Molecular Weight:423.301
Hs Code.:

Synonyms:5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

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Chemical Property of 5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

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Technology Process of 5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

There total 4 articles about 5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 879015-65-3
1,3-bis(allyloxy)-2-allyloxymethyl-2-[(p-bromophenoxy)methyl]propane

: 879015-67-5
5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

Guidance literature:: 1,3-bis(allyloxy)-2-allyloxymethyl-2-[(p-bromophenoxy)methyl]propane; With ozone; In methanol; dichloromethane; at -78 ℃;

With dimethylsulfide; In methanol; dichloromethane; at -78 - 20 ℃;

With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃;
DOI:10.1021/jo052045u

Reference yield:

: 879015-64-2
1,3-bis(allyloxy)-2-allyloxymethyl-2-[(p-toluenesulfonyloxy)methyl]propane

: 879015-67-5
5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 70 percent / NaOH / dimethylformamide / 12 h / Heating

2.1: ozone / CH₂Cl₂; methanol / -78 °C

2.2: dimethyl sulfide / CH₂Cl₂; methanol / -78 - 20 °C

2.3: 81 percent / sodium borohydride / ethanol / 0 - 20 °C

With sodium hydroxide; ozone; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052045u

Reference yield:

: 106-41-2
4-bromo-phenol

: 879015-67-5
5-[(p-bromophenoxy)methyl]-5-[(2-hydroxyethoxy)methyl]-3,7-dioxa-1,9-nonanediol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 70 percent / NaOH / dimethylformamide / 12 h / Heating

2.1: ozone / CH₂Cl₂; methanol / -78 °C

2.2: dimethyl sulfide / CH₂Cl₂; methanol / -78 - 20 °C

2.3: 81 percent / sodium borohydride / ethanol / 0 - 20 °C

With sodium hydroxide; ozone; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052045u