6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether

Base Information

• Chemical Name: 6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether
• CAS No.: 107612-20-4
• Molecular Formula: C₃₂H₃₄O₃
• Molecular Weight: 466.62

Synonyms:6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether

Chemical Property of 6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether

Chemical Property:

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Technology Process of 6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether

There total 1 articles about 6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(8R,9S,13S,14S,17S)-6-(4-Benzyloxy-phenyl)-3-methoxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthrene-6,17-diol (107612-18-0,107612-19-1) → 6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether (107612-20-4)

Guidance literature:

With hydrogenchloride; In methanol; for 0.5h; Heating;

Reference yield:

6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether (107612-20-4) → 6β-(p-Hydroxyphenyl)-estra-1,3,5(10)-triene-3,17β-diol 3-methyl ether (107612-22-6)

Guidance literature:

With hydrogen; nickel; In methanol; for 6h; under 2585.7 Torr;

Reference yield:

6-(p-Benzyloxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether (107612-20-4) → 6-(p-Hydroxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether (107612-21-5)

Guidance literature:

With hydrogen; diethylamine; nickel; In methanol; for 2h; Ambient temperature;

upstream raw materials:

(8R,9S,13S,14S,17S)-6-(4-Benzyloxy-phenyl)-3-methoxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthrene-6,17-diol

Downstream raw materials:

6-(p-Hydroxyphenyl)-estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether

6β-(p-Hydroxyphenyl)-estra-1,3,5(10)-triene-3,17β-diol 3-methyl ether

6β--estra-1,3,5(10),6-tetraene-3,17β-diol 3-methyl ether hydrochloride

6β--estra-1,3,5(10)-triene-3,17β-diol 3-methyl ether hydrochloride

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