(S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one

Base Information

Chemical Name:(S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one
CAS No.:947231-52-9
Molecular Formula:C₂₃H₃₃NO₅S
Molecular Weight:435.585
Hs Code.:

Synonyms:(S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one

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Technology Process of (S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one

There total 1 articles about (S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 886733-92-2
S-3,3-dimethoxypropyl methanethiosulfonate

: (S)-4-benzyl-3-(2-methylhept-2-enoyl)oxazolidin-2-one

: C₂₃H₃₃NO₅S

: 947231-52-9
(S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one

: C₂₃H₃₃NO₅S

Guidance literature:: (S)-4-benzyl-3-(2-methylhept-2-enoyl)oxazolidin-2-one; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; Inert atmosphere;

S-3,3-dimethoxypropyl methanethiosulfonate; In tetrahydrofuran; toluene; at -78 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1248/cpb.57.920

Reference yield: 96.0%

: 947231-52-9
(S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one

: 100-51-6,185532-71-2
benzyl alcohol

: 947231-58-5
(R,E)-benzyl 2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoate

Guidance literature:: benzyl alcohol; With titanium(IV)isopropoxide; at 20 ℃; for 5h; under 0.5 - 1 Torr; Inert atmosphere;

(S)-4-benzyl-3-[(R,E)-2-(3,3-dimethoxypropylthio)-2-methylhept-3-enoyl]oxazolidin-2-one; at 70 ℃; for 16h; Inert atmosphere;
DOI:10.1248/cpb.57.920