2-(5-Ethenyltetrahydro-5-methylfuran-2-yl)-4,4-dimethyl-5-hexen-3-one

Base Information

Chemical Name:2-(5-Ethenyltetrahydro-5-methylfuran-2-yl)-4,4-dimethyl-5-hexen-3-one
CAS No.:30925-48-5
Molecular Formula:C₁₅H₂₄O₂
Molecular Weight:236.354
Hs Code.:
Mol file:30925-48-5.mol

Synonyms:5-Hexen-3-one,2-(5-ethenyltetrahydro-5-methyl-2-furanyl)-4,4-dimethyl-, [2S-[2a(R*),5a]]-; Artemone

Suppliers and Price of 2-(5-Ethenyltetrahydro-5-methylfuran-2-yl)-4,4-dimethyl-5-hexen-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(5-Ethenyltetrahydro-5-methylfuran-2-yl)-4,4-dimethyl-5-hexen-3-one

Chemical Property:

Vapor Pressure:0.00108mmHg at 25°C
Boiling Point:301°Cat760mmHg
Flash Point:107.3°C
PSA：26.30000
Density:0.96g/cm³
LogP:3.52750

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(5-Ethenyltetrahydro-5-methylfuran-2-yl)-4,4-dimethyl-5-hexen-3-one

There total 9 articles about 2-(5-Ethenyltetrahydro-5-methylfuran-2-yl)-4,4-dimethyl-5-hexen-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 113729-62-7
(2R,5S)-5-{(S)-1-[2-(1,1-Dimethyl-allyl)-[1,3]dithian-2-yl]-ethyl}-2-methyl-2-vinyl-tetrahydro-furan

: 30925-48-5
(+)-artemone

Guidance literature:: With N-chloro-succinimide; silver nitrate; In water; acetone; acetonitrile; at 0 ℃;
DOI:10.1246/cl.1987.1259

Reference yield: 57.0%

: 4,4-dimethyl-2-(5-methyl-5-vinyltetrahydrofuran-2-yl)hex-5-en-3-ol

: 30925-48-5
(+)-artemone

Guidance literature:: With sulfur trioxide pyridine complex; In dichloromethane; dimethyl sulfoxide; at 20 ℃; for 48h;
DOI:10.1055/s-0034-1380684

Reference yield: 49.0%

: 1150633-81-0
ethyl (2S)-2-[(2S,5S)-5-methyl-5-vinyltetrahydrofuran-2-yl]propanoate

: 503-60-6
3,3-dimethyl-allyl chloride

: 30925-48-5
(+)-artemone

Guidance literature:: 3,3-dimethyl-allyl chloride; With magnesium; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

ethyl (2S)-2-[(2S,5S)-5-methyl-5-vinyltetrahydrofuran-2-yl]propanoate; In tetrahydrofuran; at -78 ℃; for 21.25h; Inert atmosphere;
DOI:10.1055/s-0033-1338429