10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol

Base Information

Chemical Name:10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol
CAS No.:177364-26-0
Molecular Formula:C₂₆H₄₀O₂Si₂
Molecular Weight:440.773
Hs Code.:

Synonyms:10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol

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Chemical Property of 10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol

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Technology Process of 10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol

There total 2 articles about 10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 54655-07-1
lithium trimethylsilylacetylenide

: 177364-24-8
8-(tert-Butyl-dimethyl-silanyloxy)-2-[1-phenyl-meth-(E)-ylidene]-oct-3-ynal

: 177364-26-0
10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol

Guidance literature:: In tetrahydrofuran; at -80 ℃; for 0.5h;

Reference yield:

: 8-Hydroxy-2-[1-phenyl-meth-(E)-ylidene]-oct-3-ynal

: 177364-26-0
10-(tert-Butyl-dimethyl-silanyloxy)-4-[1-phenyl-meth-(E)-ylidene]-1-trimethylsilanyl-deca-1,5-diyn-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 24 h / 20 °C

2: 74 percent / tetrahydrofuran / 0.5 h / -80 °C

With 1H-imidazole; In tetrahydrofuran; N,N-dimethyl-formamide;