2-hydroxy-N-(pyridin-2-ylmethyl)benzamide

Base Information

• Chemical Name: 2-hydroxy-N-(pyridin-2-ylmethyl)benzamide
• CAS No.: 57786-42-2
• Molecular Formula: C₁₃H₁₂N₂O₂
• Molecular Weight: 228.25
• European Community (EC) Number: 882-036-4
• Nikkaji Number: J2.646.478A
• Mol file: 57786-42-2.mol

Synonyms:2-hydroxy-N-(pyridin-2-ylmethyl)benzamide;57786-42-2;2-hydroxy-N-[(pyridin-2-yl)methyl]benzamide;CBKinase1_010882;CBKinase1_023282;Oprea1_733617;SCHEMBL9202857;N-(2-pyridylmethyl)salicylamide;UETKAFXUXVMKPJ-UHFFFAOYSA-N;MFCD03408079;STK735450;AKOS000211685;SB80430;2-Hydroxy-N-pyridin-2-ylmethyl-benzamide;LS-09018;EU-0086176;EN300-315600;SR-01000534952;SR-01000534952-1;BRD-K66037674-001-01-1

Chemical Property of 2-hydroxy-N-(pyridin-2-ylmethyl)benzamide

Chemical Property:

• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 228.089877630
• Heavy Atom Count: 17
• Complexity: 258

Purity/Quality:

99% ^*data from raw suppliers

2-Hydroxy-N-(pyridin-2-ylmethyl)benzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C(=O)NCC2=CC=CC=N2)O

Technology Process of 2-hydroxy-N-(pyridin-2-ylmethyl)benzamide

There total 2 articles about 2-hydroxy-N-(pyridin-2-ylmethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

2-(Aminomethyl)pyridine (3731-51-9) + methyl salicylate (119-36-8,8024-54-2) → 2-hydroxy-N-((pyridin-2-yl)methyl)benzamide (57786-42-2)

Guidance literature:

With 1-methyl-1H-imidazole; In pentan-1-ol; at 165 ℃; for 8h; Inert atmosphere;

DOI:10.1002/zaac.201200084

Reference yield:

→ 2-hydroxy-N-((pyridin-2-yl)methyl)benzamide (57786-42-2)

Guidance literature:

Salicylsaeurechlorid, Ae., Pyridyl-(2)-methylamin;

Reference yield: 92.0%

2,5-dibromomethyl-p-xylene (35168-62-8) + 2-hydroxy-N-((pyridin-2-yl)methyl)benzamide (57786-42-2) → C36H34N4O4

Guidance literature:

2-hydroxy-N-((pyridin-2-yl)methyl)benzamide; With potassium carbonate; In acetone; at 20 ℃; for 0.5h;

2,5-dibromomethyl-p-xylene; In acetone; for 10h;

DOI:10.1002/zaac.201300531

upstream raw materials:

2-(Aminomethyl)pyridine

methyl salicylate

Downstream raw materials:

(OCH₃)2(C₁₀H₄)(CH₂O(C₆H₄)C(O)NHCH₂(C₅H₄N))2

[copper(II)(2-hydroxy-N-(2-pyridylmethyl)benzamide)2Cl₂]

1,5-bis[[(2'-(2-picolylaminoformyl))phenoxyl]methyl]naphthalene

C₃₄H₃₀N₄O₄

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