2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

Base Information

Chemical Name:2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride
CAS No.:108288-31-9
Molecular Formula:C₁₄H₁₀N₄O*ClH
Molecular Weight:286.721
Hs Code.:

Synonyms:2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

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Chemical Property of 2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

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Technology Process of 2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

There total 5 articles about 2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 108288-26-2
N-(3-Amino-pyridin-4-yl)-4-cyano-2-methoxy-benzamide

: 108288-31-9
2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

Guidance literature:: With hydrogenchloride; In ethylene glycol; at 195 ℃;
DOI:10.1016/S0040-4039(00)85382-4

Reference yield:

: 54-96-6
3,4-diaminopyridine

: 108288-31-9
2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

Guidance literature:: Multi-step reaction with 2 steps

2: 30 percent / concentrated hydrochloric acid / ethane-1,2-diol / 195 °C

With hydrogenchloride; In ethylene glycol;
DOI:10.1016/S0040-4039(00)85382-4

Reference yield:

: 2486-80-8
4-amino-2-methoxybenzoic acid

: 108288-31-9
2-(4-cyano-2-methoxyphenyl)-1H-imidazo<4,5-c>pyridine monohydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: NaNO₂, 2N HCl

2: SOCl₂

4: 30 percent / concentrated hydrochloric acid / ethane-1,2-diol / 195 °C

With hydrogenchloride; thionyl chloride; sodium nitrite; In ethylene glycol;
DOI:10.1016/S0040-4039(00)85382-4