3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate

Base Information

Chemical Name:3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate
CAS No.:257282-83-0
Molecular Formula:C₁₈H₂₆O₆S₂
Molecular Weight:402.533
Hs Code.:

Synonyms:3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate

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Chemical Property of 3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate

Chemical Property:

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Technology Process of 3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate

There total 2 articles about 3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 499-49-0
5-methylisophthalic aicd

: 257282-83-0
3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 1,1'-carbonyldiimidazole; DBU / dimethylformamide / 24 h / 40 °C

2: 96 percent / NBS; 1,1'-azobis(cyclohexanecarbonitrile) / CCl₄ / 6 h / Heating

3: 60 percent / dimethylformamide / 1 h / 50 °C

With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,1'-carbonyldiimidazole; 1,1'-azobis(1-cyanocyclohexanenitrile); In tetrachloromethane; N,N-dimethyl-formamide; 1: Esterification / 2: Bromination / 3: Alkylation;
DOI:10.1016/S0968-0896(99)00167-4

Reference yield:

: di-tert-butyl toluene-3,5-dicarboxylate

: 257282-83-0
3,5-di(tert-butoxycarbo)benzyl methanethiosulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NBS; 1,1'-azobis(cyclohexanecarbonitrile) / CCl₄ / 6 h / Heating

2: 60 percent / dimethylformamide / 1 h / 50 °C

With N-Bromosuccinimide; 1,1'-azobis(1-cyanocyclohexanenitrile); In tetrachloromethane; N,N-dimethyl-formamide; 1: Bromination / 2: Alkylation;
DOI:10.1016/S0968-0896(99)00167-4