[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide

Base Information

Chemical Name:[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide
CAS No.:728041-76-7
Molecular Formula:C₂₁H₁₇F₆NO₃S
Molecular Weight:477.427
Hs Code.:

Synonyms:[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide

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Technology Process of [2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide

There total 2 articles about [2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 170996-99-3
[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-acetyl chloride

: 103-49-1
dibenzylamine

: 728041-76-7
[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In diethyl ether; at -78 ℃; for 0.5h;
DOI:10.1055/s-2004-822341

Reference yield:

: 170996-97-1
[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]acetic acid

: 728041-76-7
[2,2-bis(trifluoromethyl)-5-oxo-1,3-oxathiolan-4-yl]-N,N-dibenzylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / SOCl₂ / 6 h / Heating

2: 67 percent / N-ethyldiisopropylamine / diethyl ether / 0.5 h / -78 °C

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In diethyl ether;
DOI:10.1055/s-2004-822341