[11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

Base Information

Chemical Name:[11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate
CAS No.:103740-91-6
Molecular Formula:C₁₇H₂₆O₂
Molecular Weight:263.381
Hs Code.:

Synonyms:[11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

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Chemical Property of [11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

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Technology Process of [11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

There total 1 articles about [11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-77-6,14901-07-6
(E)-β-ionone

: 61203-67-6
ethyl (diethoxyphosphono)-[1-¹³C]-acetate

: [11-13C]-(2Z,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

: 103740-91-6
[11-13C]-(2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate

Guidance literature:: ethyl (diethoxyphosphono)-[1-¹³C]-acetate; With sodium hydride; In diethyl ether; for 2h;

(E)-β-ionone; In diethyl ether; for 62h; optical yield given as %de;
DOI:10.1016/j.tet.2011.07.092