3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

Base Information

Chemical Name:3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline
CAS No.:1423470-06-7
Molecular Formula:C₄₂H₄₃NO₂S
Molecular Weight:625.875
Hs Code.:

Synonyms:3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

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Chemical Property of 3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

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Technology Process of 3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

There total 5 articles about 3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1423469-61-7
6-chloro-3,9-bis(4-(hexyloxy)phenyl)indolizino[6,5,4,3-ija]quinoline

: 54663-78-4
tributyl(thien-2-yl)stannane

: 1423470-06-7
3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; cesium fluoride; In 1,4-dioxane; toluene; at 100 ℃; Inert atmosphere;
DOI:10.1002/anie.201205007

Reference yield:

: 1423469-24-2
1-(2,6-dibromo-4-chlorophenyl)-1H-pyrrole

: 1423470-06-7
3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro bis(acetonitrile) palladium(II); copper(l) iodide; tri-tert-butyl phosphine; diisopropylamine / 1,4-dioxane; toluene / 20 °C / Inert atmosphere

2: indium(III) chloride / toluene / 24 h / 100 °C / Inert atmosphere

3: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cesium fluoride / 1,4-dioxane; toluene / 100 °C / Inert atmosphere

With indium(III) chloride; dichloro bis(acetonitrile) palladium(II); tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; tri-tert-butyl phosphine; diisopropylamine; cesium fluoride; In 1,4-dioxane; toluene;
DOI:10.1002/anie.201205007

Reference yield:

: 1423469-41-3
1-(4-chloro-2,6-bis((4-(hexyloxy)phenyl)ethynyl)phenyl)-1H-pyrrole

: 1423470-06-7
3,9-bis(4-(hexyloxy)phenyl)-6-(thiophen-2-yl)indolizino[6,5,4,3-ija]quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: indium(III) chloride / toluene / 24 h / 100 °C / Inert atmosphere

2: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cesium fluoride / 1,4-dioxane; toluene / 100 °C / Inert atmosphere

With indium(III) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; cesium fluoride; In 1,4-dioxane; toluene;
DOI:10.1002/anie.201205007