(2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone

Base Information

• Chemical Name: (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone
• CAS No.: 176101-72-7
• Molecular Formula: C₁₅H₁₇NO₂
• Molecular Weight: 243.305

Synonyms:(2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone

Chemical Property of (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone

Chemical Property:

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Technology Process of (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone

There total 2 articles about (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) + mesitylenecarbonitrile oxide (2904-57-6) → (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone (176101-72-7) + 3-(2,4,6-trimethyl-phenyl)-4,6a-dihydro-3aH-cyclopenta[d]isoxazole

Guidance literature:

With 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃;

DOI:10.1016/S0040-4020(99)00574-8

Reference yield: 60.0%

cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) + mesitylenecarbonitrile oxide (2904-57-6) → (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone (176101-72-7)

Guidance literature:

With 4-methylmorpholine N-oxide; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1016/0040-4039(96)00151-7

Reference yield: 48.0%

benzohydroximoyl chloride (698-16-8) + (2-Oxa-3-aza-bicyclo[2.2.1]hept-5-en-3-yl)-(2,4,6-trimethyl-phenyl)-methanone (176101-72-7) → ((1S,2S,6R,7R)-5-Phenyl-3,9-dioxa-4,8-diaza-tricyclo[5.2.1.02,6]dec-4-en-8-yl)-(2,4,6-trimethyl-phenyl)-methanone + ((1R,2R,6R,7S)-5-Phenyl-3,8-dioxa-4,9-diaza-tricyclo[5.2.1.02,6]dec-4-en-9-yl)-(2,4,6-trimethyl-phenyl)-methanone

Guidance literature:

With triethylamine; In benzene; at 20 ℃; for 48h;

DOI:10.1002/1099-0690(200007)2000:14<2613::aid-ejoc2613>3.0.co;2-7

upstream raw materials:

cyclopenta-1,3-diene

mesitylenecarbonitrile oxide

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