(S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

Base Information

Chemical Name:(S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate
CAS No.:125150-53-0
Molecular Formula:C₃₃H₃₈O₇
Molecular Weight:546.661
Hs Code.:

Synonyms:(S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

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Chemical Property of (S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

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Technology Process of (S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

There total 8 articles about (S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 125150-44-9
(S)-1-(benzyloxycarbonyl)-2-methylpropyl 4-(4'octoxybiphenyl-4-carbonyloxy)benzoate

: 125150-53-0
(S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 760 Torr;

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 125150-53-0
(S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaNO₂, 0.5 M H₂SO₄, 2.) NaOH / 1.) water, -2-0 deg C, 3 h, overnight, room temp., 2.) water, pH=4.5-5.0

2: 96 percent / dimethylformamide / 24 h / Ambient temperature

3: 63 percent / DCC, 4-(N-pyrrolidino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

4: 70 percent / hydrogen / 5percent Pd-on charcoal / ethyl acetate / 760 Torr

With sodium hydroxide; sulfuric acid; hydrogen; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; sodium nitrite; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 59748-18-4
4'-octyloxy(1,1'-biphenyl)-4-carboxylic acid

: 125150-53-0
(S)-1-carboxy-2-methylpropyl 4-(4'-octoxybiphenyl-4-carbonyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / DCC, 4-(N-pyrrolidino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

2: 96 percent / hydrogen / 5percent Pd-on charcoal / ethyl acetate

3: 63 percent / DCC, 4-(N-pyrrolidino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

4: 70 percent / hydrogen / 5percent Pd-on charcoal / ethyl acetate / 760 Torr

With hydrogen; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; ethyl acetate;