N₁-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride

Base Information

• Chemical Name: N₁-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride
• CAS No.: 878631-09-5
• Molecular Formula: C₂₀H₃₀N₄O₃S*ClH
• Molecular Weight: 443.01

Synonyms:N₁-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride

Chemical Property of N₁-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride

Chemical Property:

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Technology Process of N₁-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride

There total 1 articles about N₁-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,1-dimethylethyl {(1S)-1-[({1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}amino)carbonyl]-3-methylbutyl}carbamate (878631-08-4) → N1-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride (878631-09-5)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane;

Reference yield:

benzo[b]thiophene-2-carboxylic acid (6314-28-9) + N1-{1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}-L-leucinamide hydrochloride (878631-09-5) → C29H34N4O4S2 + C29H34N4O4S2

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

upstream raw materials:

1,1-dimethylethyl {(1S)-1-[({1-[(2-cyanophenyl)sulfonyl]-4-methylhexahydro-1H-azepin-4-yl}amino)carbonyl]-3-methylbutyl}carbamate

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