1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole

Base Information

• Chemical Name: 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole
• CAS No.: 128997-54-6
• Molecular Formula: C₁₈H₁₆ClN₃OS
• Molecular Weight: 357.864

Synonyms:1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole

Chemical Property of 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole

Chemical Property:

Purity/Quality:

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Technology Process of 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole

There total 3 articles about 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-1,2-dihydro-[1,2,4]triazole-3-thione (128997-67-1) + dimethyl sulfate (77-78-1) → 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole (128997-54-6)

Guidance literature:

With potassium carbonate; In acetone; for 3h; Heating;

DOI:10.1016/S0040-4020(01)81434-4

Reference yield:

4-Methoxyzimtsaeurechlorid (261920-13-2) → 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole (128997-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) NaOH / 1.) benzene, 80 deg C, 90 min, 2.) 25percent methanol, 50 deg C

2: 86 percent / NaOH / methanol; H₂O / 1.5 h / Heating

With sodium hydroxide; In methanol; water;

DOI:10.1016/0223-5234(90)90015-U

Reference yield:

p-chlorophenyl thiosemicarbazide (7382-41-4) → 1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-3-methylsulfanyl-1H-[1,2,4]triazole (128997-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) NaOH / 1.) benzene, 80 deg C, 90 min, 2.) 25percent methanol, 50 deg C

2: 86 percent / NaOH / methanol; H₂O / 1.5 h / Heating

With sodium hydroxide; In methanol; water;

DOI:10.1016/0223-5234(90)90015-U

upstream raw materials:

1-(4-Chloro-phenyl)-5-[(Z)-2-(4-methoxy-phenyl)-vinyl]-1,2-dihydro-[1,2,4]triazole-3-thione

dimethyl sulfate

4-Methoxyzimtsaeurechlorid

p-chlorophenyl thiosemicarbazide

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