2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

Base Information

Chemical Name:2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside
CAS No.:1381952-69-7
Molecular Formula:C₂₂H₂₆N₂O₅
Molecular Weight:398.459
Hs Code.:

Synonyms:2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

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Chemical Property of 2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

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Technology Process of 2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

There total 6 articles about 2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: C₂₂H₂₄N₄O₅

: 1381952-69-7
2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/acsmedchemlett.5b00214

Reference yield:

: 1078691-95-8
(+)-D-glucosamine hydrochloride

: 1381952-69-7
2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / Reflux

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane

2.2: 20 °C

3.1: boron trifluoride diethyl etherate / 18 h / 80 °C

4.1: pyridine / 3 h / 20 °C

5.1: sodium azide / N,N-dimethyl-formamide / 90 °C

6.1: triphenylphosphine / water; tetrahydrofuran / 20 °C

With pyridine; sodium azide; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.5b00214

Reference yield:

: C₂₉H₃₁NO₈S

: 1381952-69-7
2-propen-1-yl 6-amino-2-[(3-biphenylcarbonyl)amino]-2,6-dideoxy-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 90 °C

2: triphenylphosphine / water; tetrahydrofuran / 20 °C

With sodium azide; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/acsmedchemlett.5b00214