bis(3-salicylideneaminopropyl)-p-tolylamine

Base Information

• Chemical Name: bis(3-salicylideneaminopropyl)-p-tolylamine
• CAS No.: 1174291-71-4
• Molecular Formula: C₂₈H₃₃N₃O₂
• Molecular Weight: 443.589
• Mol file: 1174291-71-4.mol

Synonyms:bis(3-salicylideneaminopropyl)-p-tolylamine

Chemical Property of bis(3-salicylideneaminopropyl)-p-tolylamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of bis(3-salicylideneaminopropyl)-p-tolylamine

There total 1 articles about bis(3-salicylideneaminopropyl)-p-tolylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

4-Methylbenzyl bromide (104-81-4) + 2,2'-(((azanediylbis(propane-3,1-diyl))bis(azanylylidene))bis(methanylylidene))diphenol → bis(3-salicylideneaminopropyl)-p-tolylamine (1174291-71-4)

Guidance literature:

With potassium carbonate; potassium iodide; In acetonitrile; Reflux;

DOI:10.1002/ejic.200800227

Reference yield: 40.0%

ammonium thiocyanate + Iron(III) nitrate nonahydrate + bis(3-salicylideneaminopropyl)-p-tolylamine (1174291-71-4) → [(bis(3-salicylideneaminopropyl)-p-tolylamine(2-))Fe(NCS)]

Guidance literature:

With CH₃ONa; In ethanol; soln. of Fe(NO3)3*9H2O and NH4NCS in EtOH added to soln. of ligand and MeONa in EtOH, mixt. stirred at room temp. for 30 min; crystn. on slow evapn.; elem. anal.;

DOI:10.1002/ejic.200800227

upstream raw materials:

4-Methylbenzyl bromide