Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester

Base Information

Chemical Name:Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester
CAS No.:99560-27-7
Molecular Formula:C₁₆H₁₄ClF₆NO₄
Molecular Weight:433.735
Hs Code.:

Synonyms:Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester

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Chemical Property of Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester

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Technology Process of Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester

There total 2 articles about Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 99560-26-6
(E)-3-<4-chloro-3-methoxy-5-(methylamino)phenyl>-2-methyl-2-propen-1-ol

: 407-25-0
trifluoroacetic anhydride

: 99560-27-7
Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester

Guidance literature:: With sodium carbonate; In diethyl ether; for 0.5h;
DOI:10.1021/jo00350a098

Reference yield:

: 99560-38-0
(E)-3-<4-chloro-3-methoxy-5-(methylamino)phenyl>-2-methyl-2-propenal

: 99560-27-7
Trifluoro-acetic acid (E)-3-{4-chloro-3-methoxy-5-[methyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-2-methyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / NaBH₄ / methanol / 3 h / 0 - 5 °C

2: 98 percent / Na₂CO₃ / diethyl ether / 0.5 h

With sodium tetrahydroborate; sodium carbonate; In methanol; diethyl ether;
DOI:10.1021/jo00350a098