N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide

Base Information

Chemical Name:N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide
CAS No.:1637586-70-9
Molecular Formula:C₂₂H₂₅F₄N₅O₂
Molecular Weight:467.466
Hs Code.:

Synonyms:N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide

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Technology Process of N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide

There total 2 articles about N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1637586-61-8
C₃₂H₄₁F₄N₅O₆

: 1637586-70-9
N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.3390/molecules19056163

Reference yield:

: 1637586-56-1
C₂₁H₂₃F₄N₃O₂

: 1637586-70-9
N-(1-(4-guanidinobenzyl)piperidin-4-yl)-3-(1,1,2,2-tetrafluoroethoxy)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: mercury dichloride; triethylamine / dichloromethane / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

With triethylamine; trifluoroacetic acid; mercury dichloride; In dichloromethane;
DOI:10.3390/molecules19056163