2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

Base Information

Chemical Name:2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate
CAS No.:1257226-99-5
Molecular Formula:C₆₅H₇₆O₁₀S₃
Molecular Weight:1113.51
Hs Code.:

Synonyms:2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

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Chemical Property of 2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

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Technology Process of 2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

There total 6 articles about 2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.3%

: 1257226-98-4
3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoic acid

: 273400-09-2
2-(2,5-di(thiophen-2-yl)thiophene-3-yl)ethanol

: 1257226-99-5
2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ma101746e

Reference yield:

: 1257226-93-9
methyl 3,4,5-tris(pent-4-enyloxy)benzoate

: 1257226-99-5
2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 5 - 20 °C / Inert atmosphere; Sonication

3: water; potassium hydroxide / tetrahydrofuran; ethanol / 24 h / 80 °C / Inert atmosphere

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; water; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; 2: Mitsunobu reaction;
DOI:10.1021/ma101746e

Reference yield:

: 1257226-94-0
(3,4,5-tris(pent-4-enyloxy)phenyl)methanol

: 1257226-99-5
2-(2,5-di(thiophen-2-yl)thiophen-3-yl)ethyl 3,5-bis(3,4,5-tris(pent-4-enyloxy)benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 5 - 20 °C / Inert atmosphere; Sonication

2: water; potassium hydroxide / tetrahydrofuran; ethanol / 24 h / 80 °C / Inert atmosphere

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; di-isopropyl azodicarboxylate; water; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; 1: Mitsunobu reaction;
DOI:10.1021/ma101746e