[trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

Base Information

Chemical Name:[trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]
CAS No.:875439-39-7
Molecular Formula:CF₃O₃S*C₃₆H₆₆N₅P₂Pd
Molecular Weight:886.391
Hs Code.:

Synonyms:[trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

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Chemical Property of [trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

Chemical Property:

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Technology Process of [trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

There total 5 articles about [trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 875439-23-9
trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(triflate)

: 100-46-9
benzylamine

: 875439-39-7
[trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

Guidance literature:: In dichloromethane; under dry N2 atm. using Schlenk line and glovebox techniques; Pd complexdissolved in CH2Cl2; benzylamine added; mixt. stirred at room temp. for 24 h; soln. concd. to dryness; solid recrystd. by slowly diffusing Et2O into CH2Cl2 soln.; crystals washed (cold Et2O); dried (vac.); elem. anal.;
DOI:10.1021/ja054779u

Reference yield:

: 875439-13-7
4-(tert-butyl)-2-(diisopropylphosphino)-1-methyl-1H-imidazole

: 875439-39-7
[trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

Guidance literature:: Multi-step reaction with 3 steps

1: benzene

2: benzene

3: dichloromethane

In dichloromethane; benzene;
DOI:10.1021/ja054779u

Reference yield:

: 875439-19-3
bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)palladium⁽⁰⁾

: 875439-39-7
[trans-bis(di-isopropyl-(1-methyl-4-tert-butylimidazol-2-yl)phosphine)Pd(methyl)(benzylamine)][triflate]

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: dichloromethane

In dichloromethane; benzene;
DOI:10.1021/ja054779u