2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Base Information

Chemical Name:2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid
CAS No.:96043-05-9
Molecular Formula:C₃₄H₃₆ClN₃O₁₅
Molecular Weight:762.124
Hs Code.:

Synonyms:2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Suppliers and Price of 2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

There total 3 articles about 2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 87376-57-6
2-azido-4,6-di-O-benzoyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyl bromide

: 96043-05-9
2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Guidance literature:: With tetraethylammonium chloride; In acetonitrile;
DOI:10.1016/0008-6215(84)85006-5

Reference yield:

: 87376-56-5
1-Acetyl-2-azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-O-α-D-galactopyranose

: 96043-05-9
2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / 6 h / 20 °C

2: 79 percent / tetraethylammonium chloride / acetonitrile

With tetraethylammonium chloride; titanium(IV) bromide; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/0008-6215(84)85006-5

Reference yield:

: Methyl-2-azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosid

: 96043-05-9
2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / H₂SO₄ / 12 h / -20 °C

2: 97 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / 6 h / 20 °C

3: 79 percent / tetraethylammonium chloride / acetonitrile

With sulfuric acid; tetraethylammonium chloride; titanium(IV) bromide; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/0008-6215(84)85006-5