Technology Process of C2H4O2*C17H28N3O4P
There total 5 articles about C2H4O2*C17H28N3O4P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium over charcoal;
In
ethanol;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / 65 °C
2.1: dichloromethane / 1 h / -20 °C
3.1: ozone; triphenylphosphine / dichloromethane / 1 h / -78 - 20 °C
4.1: acetic acid / ethanol / 1.5 h / 20 °C / Molecular sieve
4.2: 1 h / 20 °C
5.1: hydrogen / palladium over charcoal / ethanol / 2 h / 20 °C
With
thionyl chloride; hydrogen; ozone; acetic acid; triphenylphosphine;
palladium over charcoal;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dichloromethane / 1 h / -20 °C
2.1: ozone; triphenylphosphine / dichloromethane / 1 h / -78 - 20 °C
3.1: acetic acid / ethanol / 1.5 h / 20 °C / Molecular sieve
3.2: 1 h / 20 °C
4.1: hydrogen / palladium over charcoal / ethanol / 2 h / 20 °C
With
hydrogen; ozone; acetic acid; triphenylphosphine;
palladium over charcoal;
In
ethanol; dichloromethane;
