9R-phenylsulfanylmethylcinchonine

Base Information

Chemical Name:9R-phenylsulfanylmethylcinchonine
CAS No.:1431257-69-0
Molecular Formula:C₂₆H₂₈N₂OS
Molecular Weight:416.587
Hs Code.:

Synonyms:9R-phenylsulfanylmethylcinchonine

Suppliers and Price of 9R-phenylsulfanylmethylcinchonine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9R-phenylsulfanylmethylcinchonine

Chemical Property:

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Technology Process of 9R-phenylsulfanylmethylcinchonine

There total 3 articles about 9R-phenylsulfanylmethylcinchonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1431257-65-6
9R-epoxymethylcinchonine

: 108-98-5
thiophenol

: 1431257-69-0
9R-phenylsulfanylmethylcinchonine

Guidance literature:: With sodium hydroxide; In ethanol; at 20 ℃; for 18h;
DOI:10.1021/jo400465a

Reference yield:

: 1397202-05-9
cinchoninone

: 1431257-69-0
9R-phenylsulfanylmethylcinchonine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dimethyl sulfoxide / 52 h

2: sodium hydroxide / ethanol / 18 h / 20 °C

With potassium hydroxide; sodium hydroxide; In ethanol; dimethyl sulfoxide; 1: |Corey-Tschaikosky Epoxidation;
DOI:10.1021/jo400465a

Reference yield:

: 118-10-5
Cinchonin

: 1431257-69-0
9R-phenylsulfanylmethylcinchonine

Guidance literature:: Multi-step reaction with 3 steps

2: potassium hydroxide / dimethyl sulfoxide / 52 h

3: sodium hydroxide / ethanol / 18 h / 20 °C

With potassium hydroxide; sodium hydroxide; In ethanol; dimethyl sulfoxide; 1: |Oppenauer Oxidation / 2: |Corey-Tschaikosky Epoxidation;
DOI:10.1021/jo400465a