5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

Base Information

Chemical Name:5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole
CAS No.:1448857-79-1
Molecular Formula:C₁₇H₁₃F₁₁N₂O₂
Molecular Weight:486.285
Hs Code.:

Synonyms:5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

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Chemical Property of 5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

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Technology Process of 5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

There total 3 articles about 5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 423-46-1
perfluorohexanol

: 1448857-79-1
5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 8 h / 80 °C / Inert atmosphere; Sealed tube; Microwave irradiation

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 1 h / 105 °C / Microwave irradiation; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; mineral oil; 2: |Suzuki Coupling;
DOI:10.1021/jm400287v

Reference yield:

: 1448858-01-2
5-iodo-1-methyl-2-((2,2,3,3,4,4,5,5,6,6-undecafluorohexyl)oxy)-1H-imidazole

: 5720-06-9
2-Methoxyphenylboronic acid

: 1448857-79-1
5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 105 ℃; for 1h; Microwave irradiation; Inert atmosphere;
DOI:10.1021/jm400287v

Reference yield:

: 578-57-4
2-bromoanisole

: 1448857-79-1
5-(2-methoxyphenyl)-1-methyl-2-((2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy)-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 1 h / 105 °C / Microwave irradiation; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; water; 2: |Suzuki Coupling;
DOI:10.1021/jm400287v