tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

Base Information

Chemical Name:tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate
CAS No.:735331-59-6
Molecular Formula:C₂₂H₃₄N₄O₅
Molecular Weight:434.536
Hs Code.:

Synonyms:tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

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Chemical Property of tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

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Technology Process of tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

There total 1 articles about tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 85006-25-3
N,N-di(tert-butoxycarbonyl)hydroxylamine

: 289902-97-2
2-(3,4-dimethylbenzyl)-3-hydroxypropyl azide

: 735331-59-6
tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1016/j.bmc.2004.04.040

Reference yield:

: 735331-59-6
tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

: 735331-60-9
N-[3-azido-2-(3,4-dimethylbenzyl)propyl]hydroxylamine

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 0.333333h;
DOI:10.1016/j.bmc.2004.04.040

Reference yield:

: 735331-59-6
tert-butyl N-(3-azido-2-(3,4-dimethylbenzyl)propyl)-N-[(tert-butoxycarbonyl)oxy]carbamate

: 735331-61-0
N-[3-azido-2-(3,4-dimethylbenzyl)propyl]-N-hydroxy-2,2-dimethylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0.33 h / 20 °C

2: 0.333 g / sodium bicarbonate / CH₂Cl₂; H₂O / 2 h / 20 °C

With sodium hydrogencarbonate; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1016/j.bmc.2004.04.040