Technology Process of C34H39N3O3
There total 5 articles about C34H39N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(S,S)-6-benzyl-octahydro-pyrrolo[3,4-b]pyridine dihydrochloride; C20H19NO4;
With
acetic acid; triethylamine;
In
1,2-dichloro-ethane;
at 0 - 20 ℃;
for 0.5h;
With
sodium tris(acetoxy)borohydride;
In
1,2-dichloro-ethane;
at 20 ℃;
With
sodium cyanoborohydride;
In
1,2-dichloro-ethane;
at 40 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / 7 h / Reflux
2.1: thionyl chloride / 0.5 h / Reflux
2.2: 2 h / 0 - 20 °C
3.1: Jones reagent / acetone / 0.33 h / 0 - 20 °C
4.1: triethylamine; acetic acid / 1,2-dichloro-ethane / 0.5 h / 0 - 20 °C
4.2: 20 °C
4.3: 40 °C
With
thionyl chloride; Jones reagent; acetic acid; triethylamine;
In
1,2-dichloro-ethane; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: thionyl chloride / 0.5 h / Reflux
1.2: 2 h / 0 - 20 °C
2.1: Jones reagent / acetone / 0.33 h / 0 - 20 °C
3.1: triethylamine; acetic acid / 1,2-dichloro-ethane / 0.5 h / 0 - 20 °C
3.2: 20 °C
3.3: 40 °C
With
thionyl chloride; Jones reagent; acetic acid; triethylamine;
In
1,2-dichloro-ethane; acetone;