(Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Base Information

Chemical Name:(Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester
CAS No.:606932-86-9
Molecular Formula:C₂₅H₂₂O₆
Molecular Weight:418.446
Hs Code.:

Synonyms:(Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Suppliers and Price of (Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

There total 5 articles about (Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 459-57-4
4-fluorobenzaldehyde

: 606932-85-8
(Z)-3-(3,5-dimethoxyphenyl)-2-(4-hydroxyphenyl)acrylic acid methyl ester

: 606932-86-9
(Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 80 ℃; for 18h;
DOI:10.1016/S0968-0896(03)00393-6

Reference yield: 74.0%

: 606932-86-9
(Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Guidance literature:

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 606932-86-9
(Z)-3-(3,5-dimethoxyphenyl)-2-[4-(4-formylphenoxy)phenyl]acrylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 47 percent / acetic anhydride; triethylamine / 6 h / 130 - 140 °C

2: 13 percent / acetic anhydride; triethylamine / 24 h / 125 °C

3: 35 percent / sulfuric acid / 18 h / Heating

4: 74 percent / sodium hydride / dimethylformamide / 18 h / 80 °C

With sulfuric acid; acetic anhydride; sodium hydride; triethylamine; In N,N-dimethyl-formamide; 1: Perkin condensation;
DOI:10.1016/S0968-0896(03)00393-6