2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione

Base Information

Chemical Name:2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione
CAS No.:1430119-61-1
Molecular Formula:C₂₆H₂₇NO₃Si
Molecular Weight:434.552
Hs Code.:

2-tert-butyldiphenylsilyloxy[<sup>2</sup>H<sub>4</sub>]ethyl 1H-[<sup>15</sup>N]isoindole-1,3(2H)-dione

Synonyms:2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione

Chemical Property:

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Technology Process of 2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione

There total 2 articles about 2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430119-59-7
2-tert-butyldiphenylsilyloxy[²H₄]ethanol

: 1430119-61-1
2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; trimethylamine hydrochloride / acetonitrile / 1 h / 0 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 2 h / Reflux; Inert atmosphere

With trimethylamine hydrochloride; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2013.03.043

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1430119-61-1
2-tert-butyldiphenylsilyloxy[²H₄]ethyl 1H-[¹⁵N]isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / Reflux; Inert atmosphere

1.2: 16 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine; trimethylamine hydrochloride / acetonitrile / 1 h / 0 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide / 2 h / Reflux; Inert atmosphere

With trimethylamine hydrochloride; sodium hydride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.tet.2013.03.043