1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

Base Information

Chemical Name:1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene
CAS No.:118298-01-4
Molecular Formula:C₃₃H₄₀O₆
Molecular Weight:532.677
Hs Code.:

Synonyms:1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

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Chemical Property of 1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

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Technology Process of 1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

There total 3 articles about 1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58045-93-5
cis-1,2-Di-(3,4-dimethoxyphenyl)-anti-cis-3,4-dimethylcyclobutane

: 118298-01-4
1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent Chromat_. / Na₂CO₃, tris(p-bromophenyl)aminium hexachloroantimonate / CH₂Cl₂ / 15 h / Ambient temperature

2: 14 percent Chromat_. / Na₂CO₃, tris(p-bromophenyl)aminium hexachloroantimonate / CH₂Cl₂ / 16 h / Ambient temperature

With sodium carbonate; tris-(4-bromophenyl)aminium hexachloroantimonate; In dichloromethane;
DOI:10.1021/ja00187a029

Reference yield:

: 6379-72-2
1,2-dimethoxy-4-(E)-propenylbenzene

: 62211-17-0
1α-(3,4-Dimethoxyphenyl)-2β-methyl-3β-ethyl-5,6-dimethoxyindan

: 118298-01-4
1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

: 118298-02-5
1α,4β-Di-(3,4-dimethoxyphenyl)-2β,3α,5α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

: 118353-39-2
1β,4β-Di-(3,4-dimethoxyphenyl)-2α,3α,5α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

Guidance literature:: With sodium carbonate; tris-(4-bromophenyl)aminium hexachloroantimonate; In dichloromethane; for 16h; Further byproducts given; Ambient temperature;
DOI:10.1021/ja00187a029

Reference yield:

: 6379-72-2
1,2-dimethoxy-4-(E)-propenylbenzene

: 118298-00-3
2-(3,4-Dimethoxyphenyl)-6,7-dimethoxy-1,3-dimethylnaphthalene

: 62211-17-0
1α-(3,4-Dimethoxyphenyl)-2β-methyl-3β-ethyl-5,6-dimethoxyindan

: 118298-01-4
1α,5α-Di-(3,4-dimethoxyphenyl)-2β,3α,4β-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

: 118298-02-5
1α,4β-Di-(3,4-dimethoxyphenyl)-2β,3α,5α-trimethyl-7,8-dimethoxy-1,2,2a(Hα),3,4,5-hexahydroacenaphthylene

Guidance literature:: With sodium carbonate; tris-(4-bromophenyl)aminium hexachloroantimonate; In dichloromethane; for 16h; Further byproducts given; Ambient temperature;
DOI:10.1021/ja00187a029