N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide

Base Information

Chemical Name:N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide
CAS No.:459831-73-3
Molecular Formula:C₁₉H₂₉NO₃S₂
Molecular Weight:383.576
Hs Code.:

Synonyms:N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide

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Technology Process of N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide

There total 2 articles about N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 39098-91-4
2,2-bis(ethylthio)acetyl chloride

: 10433-32-6
4-(3-aza-4-methylpent-3-enyl)-1,2-dimethoxybenzene

: 459831-73-3
N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide

Guidance literature:: With pyridine; In dichloromethane; for 2h;
DOI:10.1021/jo020083x

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 459831-73-3
N-[2-(3,4-dimethoxyphenyl)ethyl]-2-bis(ethylsulfenyl)-N-isopropenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / molecular sieves 4 Angstroem / benzene / 24 h / 20 °C

2: 65 percent / pyridine / CH₂Cl₂ / 2 h

With pyridine; 4 A molecular sieve; In dichloromethane; benzene;
DOI:10.1021/jo020083x