6-Hydroxy-2-naphthyl disulfide

Base Information

• Chemical Name: 6-Hydroxy-2-naphthyl disulfide
• CAS No.: 6088-51-3
• Molecular Formula: C20H14 O2 S2
• Molecular Weight: 350.462
• Hs Code.: 2930909090
• European Community (EC) Number: 228-025-4
• NSC Number: 87629
• UNII: Y4YW3C2D2S
• DSSTox Substance ID: DTXSID7025429
• Nikkaji Number: J208.301I
• Wikidata: Q27294275
• ChEMBL ID: CHEMBL1489064
• Mol file: 6088-51-3.mol

Synonyms:2,2'-dihydroxy-6,6'-dinaphthyldisulfide

Chemical Property of 6-Hydroxy-2-naphthyl disulfide

Chemical Property:

• Vapor Pressure: 7.18E-15mmHg at 25°C
• Melting Point: 226 °C
• Boiling Point: 597.5°C at 760 mmHg
• PKA: 8.93±0.40(Predicted)
• Flash Point: 289.3°C
• PSA: 91.06000
• Density: 1.46g/cm³
• LogP: 6.20360
• Storage Temp.: −20°C
• XLogP3: 5.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 350.04352203
• Heavy Atom Count: 24
• Complexity: 380

Purity/Quality:

98% ^*data from raw suppliers

PIR 3.5 ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC2=C(C=CC(=C2)SSC3=CC4=C(C=C3)C=C(C=C4)O)C=C1O
• Description: DDD, 1,1-dichloro-2,2-bis-(4-chlorophenyl) ethane, also known as TDE, is a metabolite of DDT, which found use in agriculture. As with DDT, the p,p -isomer is insecticidal and the o,p -isomer is an impurity.
• Uses: For determination of protein-bound sulfhydryl groups.

Technology Process of 6-Hydroxy-2-naphthyl disulfide

There total 6 articles about 6-Hydroxy-2-naphthyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

→ 6-hydroxy-2-naphthyldisulphide (6088-51-3)

Guidance literature:

Reference yield:

carbonic acid ethyl ester-[6-(6-hydroxy-[2]naphthyldisulfanyl)-[2]naphthyl ester] → 6-hydroxy-2-naphthyldisulphide (6088-51-3)

Guidance literature:

With potassium hydroxide;

Reference yield:

6-<(ethoxycarbonyl)oxy>-2-mercaptonaphthalene (125518-82-3) → 6-hydroxy-2-naphthyldisulphide (6088-51-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; aqueous FeCl₃

2: aqueous KOH

With potassium hydroxide; ethanol; iron(III) chloride;

upstream raw materials:

(6-Oxy-naphthyl-⁽²⁾)-mercaptan

6-<(ethoxycarbonyl)oxy>-2-mercaptonaphthalene