2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane

Base Information

• Chemical Name: 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane
• CAS No.: 32102-01-5
• Molecular Formula: C₉H₁₁O₃PSe
• Molecular Weight: 277.118
• Mol file: 32102-01-5.mol

Synonyms:2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane

Chemical Property of 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane

There total 3 articles about 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

Selenophosphoric acid Se-(3-hydroxy-propyl) ester O,O'-diphenyl ester → 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane (32102-01-5) + phenol (108-95-2,27073-41-2)

Guidance literature:

In xylene; for 6h; Heating;

DOI:10.1007/BF00953117

Reference yield:

2-Phenoxy-[1,3,2]dioxaphosphinane 2-selenide → 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane (32102-01-5)

Guidance literature:

With quinoclamine; tetraethylammonium iodide;

Reference yield:

diphenylselenophosphoric acid → 2-phenoxy-2-oxo-1,3,2-oxaselenophosphorinane (32102-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / 0.5 h / Heating

2: 45 percent / xylene / 6 h / Heating

In diethyl ether; xylene;

DOI:10.1007/BF00953117