1-chloro-3-isopropenyloxybenzene

Base Information

• Chemical Name: 1-chloro-3-isopropenyloxybenzene
• CAS No.: 730985-50-9
• Molecular Formula: C₉H₉ClO
• Molecular Weight: 168.623
• Mol file: 730985-50-9.mol

Synonyms:1-chloro-3-isopropenyloxybenzene

Chemical Property of 1-chloro-3-isopropenyloxybenzene

Chemical Property:

Purity/Quality:

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Technology Process of 1-chloro-3-isopropenyloxybenzene

There total 1 articles about 1-chloro-3-isopropenyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

3-chlorophenyl acetate (13031-39-5) → 1-chloro-3-isopropenyloxybenzene (730985-50-9)

Guidance literature:

In toluene; for 0.5h;

DOI:10.1021/ja0394986

Reference yield: 73.0%

acetic anhydride (108-24-7) + 1-chloro-3-isopropenyloxybenzene (730985-50-9) → 1-(3-isopropenyloxyphenyl)ethanone (730985-51-0)

Guidance literature:

1-chloro-3-isopropenyloxybenzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 3h;

acetic anhydride; In tetrahydrofuran; at -78 ℃; for 2h;

DOI:10.1021/ja0394986

Reference yield:

1-chloro-3-isopropenyloxybenzene (730985-50-9) → benzyl-[1-(3-isopropenyloxyphenyl)ethylidene]amine

Guidance literature:

Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 3 h / 20 °C

1.2: 73 percent / tetrahydrofuran / 2 h / -78 °C

2.1: benzene / 12 h

With magnesium; In tetrahydrofuran; benzene;

DOI:10.1021/ja0394986

upstream raw materials:

3-chlorophenyl acetate

Downstream raw materials:

1-(3-isopropenyloxyphenyl)ethanone