N⁴-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine

Base Information

• Chemical Name: N⁴-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine
• CAS No.: 1041364-75-3
• Molecular Formula: C₄₆H₄₇N₄O₉P
• Molecular Weight: 830.874

Synonyms:N⁴-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine

Chemical Property of N⁴-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine

Chemical Property:

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Technology Process of N⁴-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine

There total 1 articles about N⁴-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

diisopropyl ((p-tolylsulfonyl)methyl)phosphonate (120991-42-6) + N4-benzoyl-1-[(S)-2-hydroxy-3-(trityloxy)propyl]-5-(4-nitrophenyl)cytosine (1041364-64-0) → N4-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine (1041364-75-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

DOI:10.1135/cccc20070927

Reference yield: 95.0%

N4-benzoyl-1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine (1041364-75-3) → 1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine (1041364-84-4)

Guidance literature:

With ammonia; In methanol; at 4 ℃; for 24h;

DOI:10.1135/cccc20070927

upstream raw materials:

diisopropyl ((p-tolylsulfonyl)methyl)phosphonate

N⁴-benzoyl-1-[(S)-2-hydroxy-3-(trityloxy)propyl]-5-(4-nitrophenyl)cytosine

Downstream raw materials:

1-{(S)-2-[(diisopropoxyphosphoryl)methoxy]-3-(trityloxy)propyl}-5-(4-nitrophenyl)cytosine

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