(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

Base Information

Chemical Name:(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾
CAS No.:105399-78-8
Molecular Formula:C₃₂H₅₈P₂Pt
Molecular Weight:699.84
Hs Code.:

(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum<sup>(0)</sup>

Synonyms:(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

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Chemical Property of (3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

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Technology Process of (3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

There total 4 articles about (3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: cis-[bis-(dicyclohexylphosphino)ethane]hydridoneopentylplatinum(II)

: 917-92-0
3,3-Dimethylbut-1-yne

: 105399-78-8
(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

: 105373-19-1
cis-hydrido(3,3-dimethyl-1-butynyl){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

Guidance literature:: In cyclohexane; thermolysis of cis-hydridoneopentyl{bis(dicyclohexylphosphino)ethane}platinum(II) in 3,3-dimethyl-1-butyne/cyclohexane via supposed {bis(dicyclohexylphosphino)ethane}platinum(0) at 68.6°C for 3.5 h; Kinetics;
DOI:10.1021/ja00213a016

Reference yield: 39.0%

: cis-[bis-(dicyclohexylphosphino)ethane]hydridoneopentylplatinum(II)

: 917-92-0
3,3-Dimethylbut-1-yne

: 105399-78-8
(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

: 111848-51-2
cis-{(E)-3,3-dimethyl-1-butenyl}(3,3-dimethyl-1-butynyl){bis(dicyclohexylphosphino)ethane}platinum(II)

Guidance literature:: In cyclohexane; thermolysis of cis-hydridoneopentyl{bis(dicyclohexylphosphino)ethane}platinum(II) in 3,3-dimethyl-1-butyne/cyclohexane via supposed {bis(dicyclohexylphosphino)ethane}platinum(0) at 68.6°C for 270 h; Kinetics;
DOI:10.1021/ja00213a016

Reference yield: 8.0%

: 563-79-1
2,3-Dimethyl-2-butene

: cis-[bis-(dicyclohexylphosphino)ethane]hydridoneopentylplatinum(II)

: 917-92-0
3,3-Dimethylbut-1-yne

: 105399-78-8
(3,3-dimethylbutyne){bis(dicyclohexylphosphino)ethane}platinum⁽⁰⁾

Guidance literature:: In diethyl ether; cyclohexane; cis-hydridopentyl{bis(dicyclohexylphosphino)ethane}platinum(II) in 2,3-Me2-2-butene in cyclohexane vacuum-sealed, heated at 69°C for 2.5 h, opened, solvent evapd., residue dissolved in ether, 3,3-Me2-1-butyne added, stirred at room temp. for 16 h; solvent evapd., brittle solid dissolved in min. ether, equal vol. MeOH added, cooled to -10°C, 2 more recrystns.;
DOI:10.1021/ja00213a016