3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

Base Information

Chemical Name:3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate
CAS No.:1415357-91-3
Molecular Formula:C₁₆H₂₄F₃IO₄SSi
Molecular Weight:524.415
Hs Code.:

Synonyms:3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

Suppliers and Price of 3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

There total 2 articles about 3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1415357-90-2
C₁₅H₂₅IO₂Si

: 1415357-91-3
3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 0 ℃; for 1.58333h; Inert atmosphere;
DOI:10.1021/ja309978c

Reference yield:

: 1415357-94-6
2-iodo-5-isopropylbenzene-1,3-diol

: 1415357-91-3
3-((tert-butyldimethylsilyl)oxy)-2-iodo-5-isopropylphenyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 1.58 h / -78 - 0 °C / Inert atmosphere

With triethylamine; In dichloromethane;
DOI:10.1021/ja309978c