methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

Base Information

Chemical Name:methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate
CAS No.:1544663-78-6
Molecular Formula:C₂₀H₂₃IO₃
Molecular Weight:438.305
Hs Code.:

Synonyms:methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

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Chemical Property of methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

Chemical Property:

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Technology Process of methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

There total 3 articles about methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1544663-76-4
methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-2-naphthoate

: 1544663-78-6
methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

Guidance literature:: With N-iodo-succinimide; zirconium(IV) chloride; In dichloromethane; for 2h; Inert atmosphere; Reflux;

Reference yield:

: 17295-11-3
methyl 6-hydroxynaphthalene-2-carboxylate

: 1544663-78-6
methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / toluene / 0.33 h

1.2: 0 °C / Reflux

2.1: N-iodo-succinimide; zirconium(IV) chloride / dichloromethane / 2 h / Inert atmosphere; Reflux

With N-iodo-succinimide; zirconium(IV) chloride; triphenylphosphine; In dichloromethane; toluene;

Reference yield:

: 767-13-5
3,5-dimethylcyclohexanol

: 1544663-78-6
methyl 6-(((trans,trans)-3,5-dimethylcyclohexyl)oxy)-5-iodo-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / toluene / 0.33 h

1.2: 0 °C / Reflux

2.1: N-iodo-succinimide; zirconium(IV) chloride / dichloromethane / 2 h / Inert atmosphere; Reflux

With N-iodo-succinimide; zirconium(IV) chloride; triphenylphosphine; In dichloromethane; toluene;