C₁₄H₁₈BrNO₅

Base Information

Chemical Name:C₁₄H₁₈BrNO₅
CAS No.:1357394-19-4
Molecular Formula:C₁₄H₁₈BrNO₅
Molecular Weight:360.205
Hs Code.:

C<sub>14</sub>H<sub>18</sub>BrNO<sub>5</sub>

Synonyms:C₁₄H₁₈BrNO₅

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Chemical Property of C₁₄H₁₈BrNO₅

Chemical Property:

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Technology Process of C₁₄H₁₈BrNO₅

There total 3 articles about C₁₄H₁₈BrNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1357394-15-0
C₂₀H₂₉BrN₂O₄

: 1357394-19-4
C₁₄H₁₈BrNO₅

Guidance literature:: C₂₀H₂₉BrN₂O₄; With hydrogenchloride; In water; for 12h; Reflux;

With dmap; di-tert-butyl dicarbonate; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 12h;
DOI:10.1055/s-0031-1289577

Reference yield:

: 119838-44-7
tert-butoxycarbonyl-2-(tert-butyl)-3-methyl-4-oxo-1-imidazolidinecarboxylate

: 1357394-19-4
C₁₄H₁₈BrNO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: -100 °C / Inert atmosphere

2.1: hydrogenchloride / water / 12 h / Reflux

2.2: 12 h / 0 - 20 °C

With hydrogenchloride; n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; water;
DOI:10.1055/s-0031-1289577

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1357394-19-4
C₁₄H₁₈BrNO₅

Guidance literature:: Multi-step reaction with 3 steps

1.2: Daicel Chiralpak IC / Resolution of racemate

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: -100 °C / Inert atmosphere

3.1: hydrogenchloride / water / 12 h / Reflux

3.2: 12 h / 0 - 20 °C

With hydrogenchloride; n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; water;
DOI:10.1055/s-0031-1289577