1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

Base Information

Chemical Name:1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside
CAS No.:331455-87-9
Molecular Formula:C₆₈H₅₈O₁₆Se
Molecular Weight:1210.16
Hs Code.:

Synonyms:1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

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Chemical Property of 1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

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Technology Process of 1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

There total 8 articles about 1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 872050-72-1
1,2-O-(p-methylphenylseleno-4-O-benzoyl-2,3-di-O-benzyl-β-D-glucopyranosyl-6-oxybenzylidene)-3,4,6-tri-O-benzoyl-α-D-glucopyranoside

: 331455-87-9
1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

Guidance literature:: With 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 0 ℃; for 0.5h;
DOI:10.1021/ol016713j

Reference yield: 95.0%

: C₆₈H₅₈O₁₆Se

: 331455-87-9
1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

Guidance literature:: With 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1002/chem.200500126

Reference yield:

: 165877-99-6
2,3,4,6-tetra-O-Bz-β-D-glucopyranosyl bromide

: 331455-87-9
1-p-methylphenyl 2,3-di-O-benzoyl-4-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-β-D-selenoglucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 2,6-lutidine / 12 h / 20 °C

2: 95 percent / 2,6-di-tert-butylpyridine; TMSOTf / CH₂Cl₂ / 0.5 h / 0 °C

With 2,6-dimethylpyridine; 2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/chem.200500126