(E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

Base Information

Chemical Name:(E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole
CAS No.:843612-72-6
Molecular Formula:C₃₀H₁₉N₃
Molecular Weight:421.501
Hs Code.:

Synonyms:(E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

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Chemical Property of (E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

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Technology Process of (E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

There total 3 articles about (E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 140-29-4
phenylacetonitrile

: N,N'-bis(1-naphthyl)oxaldiimidoyl dichloride

: 843612-72-6
(E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h;
DOI:10.1002/ejoc.200400405

Reference yield:

: 20961-60-8
N,N'-bis(1-naphthyl)oxalamide

: 843612-72-6
(E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / PCl₅ / toluene / 4 h / Heating

2: 91 percent / LDA / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C

With phosphorus pentachloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/ejoc.200400405

Reference yield:

: 134-32-7
1-amino-naphthalene

: 843612-72-6
(E)-2-(1-cyano-1-phenylmethylidene)-3-(1-naphthylimino)-2,3-dihydro-1H-benzo[g]indole

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / toluene / 8 h / Heating

2: 63 percent / PCl₅ / toluene / 4 h / Heating

3: 91 percent / LDA / tetrahydrofuran; hexane / 1.5 h / -78 - 20 °C

With phosphorus pentachloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/ejoc.200400405