C₄₁H₄₂N₄O₄Si

Base Information

Chemical Name:C₄₁H₄₂N₄O₄Si
CAS No.:1026285-47-1
Molecular Formula:C₄₁H₄₂N₄O₄Si
Molecular Weight:682.894
Hs Code.:

C<sub>41</sub>H<sub>42</sub>N<sub>4</sub>O<sub>4</sub>Si

Synonyms:C₄₁H₄₂N₄O₄Si

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Chemical Property of C₄₁H₄₂N₄O₄Si

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Technology Process of C₄₁H₄₂N₄O₄Si

There total 8 articles about C₄₁H₄₂N₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41082-79-5
4-methoxy-1H-indole-6-carboxylic acid methyl ester

: 1026285-47-1
C₄₁H₄₂N₄O₄Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 93 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

2.1: 98 percent / NaH / tetrahydrofuran / 1 h / 20 °C

3.1: 82 percent / N-bromosuccinimide / tetrahydrofuran / -78 - 20 °C

4.1: t-BuLi / diethyl ether; pentane / 0.25 h / -78 °C

4.2: 92 percent / diethyl ether; pentane / 1 h / -78 - 20 °C

5.1: 85 percent / K₂CO₃ / ethanol; tetrahydrofuran; H₂O / 23 h / 20 °C

6.1: 85 percent / TBAF / tetrahydrofuran / 1 h / 0 °C

7.1: 76 percent / tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

8.1: CH₂Cl₂ / Heating

With N-Bromosuccinimide; lithium aluminium tetrahydride; tetrapropylammonium perruthennate; 4 A molecular sieve; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; pentane;
DOI:10.1021/jo040211c

Reference yield:

: 791807-50-6
(4-methoxy-1H-indol-6-yl)methanol

: 1026285-47-1
C₄₁H₄₂N₄O₄Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 98 percent / NaH / tetrahydrofuran / 1 h / 20 °C

2.1: 82 percent / N-bromosuccinimide / tetrahydrofuran / -78 - 20 °C

3.1: t-BuLi / diethyl ether; pentane / 0.25 h / -78 °C

3.2: 92 percent / diethyl ether; pentane / 1 h / -78 - 20 °C

4.1: 85 percent / K₂CO₃ / ethanol; tetrahydrofuran; H₂O / 23 h / 20 °C

5.1: 85 percent / TBAF / tetrahydrofuran / 1 h / 0 °C

6.1: 76 percent / tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

7.1: CH₂Cl₂ / Heating

With N-Bromosuccinimide; tetrapropylammonium perruthennate; 4 A molecular sieve; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; pentane;
DOI:10.1021/jo040211c

Reference yield:

: 791807-40-4
4-methoxy-6-triisopropylsilanyloxymethyl-1H-indole-3-carboxylic acid ethyl ester

: 1026285-47-1
C₄₁H₄₂N₄O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / TBAF / tetrahydrofuran / 1 h / 0 °C

2: 76 percent / tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

3: CH₂Cl₂ / Heating

With tetrapropylammonium perruthennate; 4 A molecular sieve; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo040211c